JOURNAL of the Tunisian Chemical Society

serving the Research, the Education and the Industry

Synthèse de nouveaux amino dibenzohétéroazépines carbonitriles à partir de 2,3-dicyanocyclohexanone

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New amino dibenzoheteroazepine carbonitriles have been synthesized by condensation of 1,5,5-trimethyl-3-oxocyclohexane-1,2-dicarbonitrile, an isophorone derivative, with the o-phenylenediamine and its analogs. Several conditions have been used to optimize the yields. The activation of the reaction by irradiation microwaves proved to be very efficient. It led to shorter times of the reaction and to rate enhancements. Moreover, the purity of the products was increased.

N. Rachiqi, S. Fkih-Tetouani, A. El Louzi

Pages 1433-1437

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