JOURNAL of the Tunisian Chemical Society

serving the Research, the Education and the Industry

Synthesis and structural study of 3-cyano-2-(ethoxycarbonyl)-N-(4- fluorobenzyl)cyclopentanammonium chloride C16H20ClFN2O2

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The salt C16H20ClFN2O2 crystallizes in the monoclinic system, space group P21/c. The parameters of the unit cell are: a = 6.038(1) Å, b = 20.140(1) Å, c = 14.180(1) Å, β = 101,00(1)° and Z = 4. The structure is built up from (C16H20FN2O2)+ cations and Cl- anions linked by N-H..Cl hydrogen bond. The organic cation has a benzyl group linked to the ammonium group (NH2)+ which is attached to a 2,3-disubstituted five membered ring.

F. Saâdi, F. Ben Amor, A. Arfaoui, A. Driss, H. Amri

Pages 89-93

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