Synthesis, structural study, IR spectroscopy characterization and ionic behavior of Ag0.62K0.38Nb4AsO13
Written by sctunisie no commentsThe Ag0.62K0.38Nb4AsO13 compound was prepared by a solid state reaction. A qualitative analysis by scanner electronic microscope (S.E.M) and infrared (I.R) spectroscopic study were made for the state. The structural study of the Ag0.62K0.38Nb4AsO13 compound shows that this material crystallizes in the orthorhombic system (space group Cmcm) and has a three dimensional framework. There are tunnels, with hexagonal section, in where Ag+ and K+ cations are located. The characteristics derived from the structural study, which support good ion mobility, have encouraged to study the ionic conductivity through the complex impedance method.
S.F. Cherif, F. Ben Amor, M.F. Zid, A. Driss, A. Madani
S.E.M analysis, I.R spectroscopy, Structural study, C.I spectroscopy
Pages 179-190