Electrochemical difluoration of 1-alkylindenes
Written by sctunisie no commentsThe electrochemical fluoroacetamidation of 1-Alkylindene (CH3CN, Et3N, 3HF), gave small amounts of difluorinated products. The electrochemical difluorination in Et3N, 3HF/CH2Cl2 have been achieved, and the difluorinated became the major products formed. The diastereoisomers obtained were identified by NMR 1H, 13C and 19F.
H. Benotmane, A. Bensadat, E. Laurent, R.Tardivel
Pages 793-801