JOURNAL of the Tunisian Chemical Society

The vanadium oxide VO₂ (B), pure and well crystallized, was prepared by hydrothermal method (48 hours, 180°C and autogenous pressure). Diol hexane-1,6-diol HO-(CH₂)₆-OH has been used to reduce, in water, crystallized V₂O₅, in the molar ratio 1:1. The product VO₂ (B) was characterized by powder X-ray diffraction, infrared spectroscopy, Paramagnetic Electronic Resonance, thermal analysis, Brunauer-Emmet-Teller technique and Scanning Electronic Microscopy.

N. Etteyeb, Z. Idoudi, N. Gharbi

hydrothermal synthesis, V₂O₅, hexane-1,6-diol, VO₂ (B) crystallized

Pages 251-258